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The high field1H and13C resonances of obacunone were established by a series of I D and 2D NMR experiments. The13C-NMR signals of the five tertiary methyl groups and all quatenary carbons were unambiguously assigned. The results confirm the stereochemical assignments at all stereogenic centres.


Rugutt, J.k.Fischer, N.H.Nauman, M.A.Schidt, T.J.Berner, D.K.[13CNMR assignments for methyls and quarternary carbons of the limonoid abacunone]13CNMR assignments for methyls and quarternary carbons of the limonoid abacunone

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